SLM打印成形CoCrMo合金牙冠的表面粗糙度和硬度优化

田杰 ,戚文军,黄正华,李亚江,刘建业 ,胡高峰

钢铁研究学报 ›› 2018, Vol. 30 ›› Issue (5) : 411-415.

钢铁研究学报 ›› 2018, Vol. 30 ›› Issue (5) : 411-415. DOI: 10. 13228/j.boyuan.issn1001- 0963. 20170191
材料研究

SLM打印成形CoCrMo合金牙冠的表面粗糙度和硬度优化

  • 田杰1,2,戚文军2,黄正华2,李亚江1,刘建业3,4,胡高峰3,4
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Optimization of surface roughness and hardness for CoCrMo alloy dental crown manufactured by selective laser melting

  • TIAN Jie1,2,QI Wen- jun2,HUANG Zheng- hua2,LI Ya- jiang1,LIU Jian- ye3,4,HU Gao- feng3,4
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摘要

为了改善选区激光熔化打印成形的CoCrMo合金牙冠的表面粗糙度和硬度,提高其与人体的适配性,分别采用了电解抛光和固溶处理方法对牙冠进行改善处理。测试了经不同电解液和电解参数抛光后的牙冠表面粗糙度以及经不同工艺固溶处理后牙冠的硬度,利用三维轮廓仪观察了抛光前后表面形貌,利用金相显微镜和扫描电子显微镜观察了微观组织。结果表明,SLM制备的CoCrMo合金牙冠在HNO3+H3PO4体系电解液中抛光效果最佳,牙冠表面粗糙度较电解抛光前降低达70%以上;牙冠经1503K固溶10h后,显微硬度可由固溶前的470HV降至350HV,与人体天然牙齿硬度相当。SLM制备的CoCrMo牙冠综合性能得到了显著的改善。

Abstract

To ameliorate the surface roughness and hardness of CoCrMo alloy dental crown fabricated by selective laser melting (SLM) for enhancing the matching suitability between SLM parts and natural teeth, electrolytic polishing and solution treatment were carried out respectively. The surface roughness of the dental crown polished by different electrolytes and electrolytic parameters, and the hardness of the dental crown solution- treated by various parameters were measured. The surface morphology of the dental crown before and after the polishing was observed by three- dimension profiler. Meanwhile, the microstructure was observed by optical microscope and scanning electron microscope. The results show that the polishing effect of the dental crown polished by HNO3 and H3PO4 solution system reaches the maximum, where the roughness decreases by 70% compared to original state. When the dental crown is solution- treated at 1503K for 10h, the hardness decreases from 470HV for no solution treatment state to 350HV, which is equivalent to the value of human natural teeth. Overall performance of CoCrMo alloy dental crown improves a lot.

关键词

牙冠 / 选区激光熔化 / CoCrMo合金 / 电解抛光 / 硬度

Key words

dental crown / selective laser melting / CoCrMo alloy / electrolytic polishing / hardness

引用本文

导出引用
田杰 ,戚文军,黄正华,李亚江,刘建业 ,胡高峰 . SLM打印成形CoCrMo合金牙冠的表面粗糙度和硬度优化[J]. 钢铁研究学报, 2018, 30(5): 411-415 https://doi.org/10. 13228/j.boyuan.issn1001- 0963. 20170191
TIAN Jie,,QI Wen- jun,HUANG Zheng- hua,LI Ya- jiang,LIU Jian- ye,,HU Gao- feng,. Optimization of surface roughness and hardness for CoCrMo alloy dental crown manufactured by selective laser melting[J]. Journal of Iron and Steel Research, 2018, 30(5): 411-415 https://doi.org/10. 13228/j.boyuan.issn1001- 0963. 20170191

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基金

广东省金属强韧化技术与应用重点实验室;广州市先进金属结构材料重点实验室;广东省重大科技专项;广东省科学院科研平台环境与能力建设专项;广东省金属材料与加工专业镇联合创新公共平台

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